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Features of ultrafiltration process engineering calculation in concentration and purification of pectin polysaccharides

https://doi.org/10.20914/2310-1202-2017-4-26-30

Abstract

In this paper, we propose a mathematical model of the process of changing the productivity of a membrane, both through the formation of a continuous gel layer, and by blocking individual pores. Also, the results of modeling the process of dia- ultrafiltration (DUF) purification of pectin solutions and their concentration by ultrafiltration (UF) using hollow fiber membranes are presented. The effect of periodic washing of the membrane and the process of gelation along the membrane on the productivity of the plant was studied. Thus, the process is characterized by two parameters, and A is the main parameter of the problem, which is the same for all stages, and the second parameter, the ratio (k =F0/F'), characterizes the degree of pore purification with a general cleaning of the membrane surface and is thus one from the characteristics of a single cycle. The valuesof a number of parameters are determined experimentally. It is shown that when the system of differential equations, represented in the normal Cauchy form describing the given technological process, is jointly solved, the productivity of the DUF system can be increased by the frequency of flushing. The conducted experiments demonstrated the advantage of the use of the DUF process in the production of pectin and the features of purification and concentration of apple and sunflower pectins in this process. It is established that the use of DUF causes the introduction of an energy-saving technological process in the production of pectin to produce the target product that meets the required quality and environmental safety of production. The introduction of the proposed methods of DUF and UF into the production of pectin leads to an improvement in the quality and cost of the product.

About the Authors

S. E. Kholov
Institute of Chemistry, Academy of Sciences of the Republic of Tajikistan
Tajikistan
Senior Researcher, Laboratory of Chemistry of High molecular compounds, Ainy str. 299/2, Dushanbe, 734063, Tajikista


K. I. Ikromi
Technological University of Tajikistan
Cand. Sci. (Engin.), associate professor, department of food technology, , N. Karabaeva str. 63/3, Dushanbe, 734061, Tajikistan


N. I. Yunusov
Technological University of Tajikistan
Cand. Sci. (Engin.), associate professor, department of automated information processing and control systems, acad. Rajabov str., Dushanbe, 734063, Tajikistan


Z. K. Mukhidinov
Institute of Chemistry, Academy of Sciences of the Republic of Tajikistan
Dr. Sci. (Chem.), professor, director, Ainy str. 299/2, Dushanbe, 734063, Tajikistan


References

1. Mukhidinov Z.K. Sposob ochistki pektinovogo gidrolizata I poluchenie pektinovogo gelya [The method of purification of pectinhydrolyzate and obtaining of pectin gel] Patent TJ, 1998. (in Russian)

2. Mulder M. Vvedenie v membrannyuy tekhnologiyu [Introduction to membrane technology] Moscow, Mir, 1999, 513 p. (in Russian)

3. Fishman M.L., Cooke P.H., Chau H.K., Coffin D.R. et al. Biomacromol, 2007, vol. 8, pp. 573.

4. Goryachiy N.V., Svittsov A.A. et al. Critical technologies. Membrany [Membranes] 2002, no. 2 (18), pp. 40–43. (in Russian)

5. Muhidinov Z.K., Dzhonmurodov A.S., Gorshkova R.M. et al. Dia-ultrafiltration concentration and purification of pectin polysaccharides. Izvestiya. Vuzov. [News of universities. Chemistry and Chemical Technology] 2011. vol. 54, no. 2. pp.121–125. (in Russian)

6. Dzhohnmurodov A.S., TeshaevKh. I., Muhidinov Z.K. at.all. Concentration and purification of pectin-containing polysaccharides on a Pilot Plandia-ultrafiltration unit. Izvestiya AN RT [News of AS of Republic of Tajikistan] 2011. vol. 142. no. 1. pp. 67–73. (in Russian)

7. Filippov A.N., Starov V.M., Lyalin  V.A. Formation of a gel layer on the membrane surface (quasistationary approximation). Khimiya I tekhnologiya vody [Chemistry and Technology of Water] 1989. vol. 11. no.  4. pp. 291–295. (in Russian)

8. Karasu K., Yoshikawa Sh., Kentish S. E., Stevens G. W. A model for cross-flow ultrafiltration of dairy whey based on the rheology of the compressible cake. Journal of Membrane Science. 2009. vol. 341. pp. 252–260.

9. Semenov A.G., Lobasenko B.A. Mathematical description of the process of ultrafiltration taking into account gel formation on the surface of the membrane.  Khranenie I pererabotka sel’khozsyriya [Storage and processing of agricultural raw materials] 2001. no.  8. pp. 15. (in Russian)


Review

For citations:


Kholov S.E., Ikromi K.I., Yunusov N.I., Mukhidinov Z.K. Features of ultrafiltration process engineering calculation in concentration and purification of pectin polysaccharides. Proceedings of the Voronezh State University of Engineering Technologies. 2017;79(4):26-30. (In Russ.) https://doi.org/10.20914/2310-1202-2017-4-26-30

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ISSN 2226-910X (Print)
ISSN 2310-1202 (Online)