Intensification of the extraction process in the production of licorice root extract
https://doi.org/10.20914/2310-1202-2024-4-185-190
Abstract
Licorice glabra (Glycyrrhiza glabra) is a perennial herbaceous plant from the legume family, widely known for its medicinal properties. Its roots contain a large number of biologically active substances, including glycyrrhizin, a compound that gives the plant a sweet taste and has many useful properties. Licorice extract is widely used in the food industry due to its unique properties: It improves the texture and consistency of products, helps to mix immiscible components as an emulsifier, and also has antimicrobial properties, extending the shelf life of products. Traditional licorice extraction methods require a long time and significant costs. This paper presents a new technology for obtaining licorice root extract based on the use of microwave exposure. The study showed that the use of microwave treatment of the extraction mixture can significantly reduce the extraction time and increase the yield of target substances. The rationalization of process parameters, such as microwave power, temperature and processing time, made it possible to achieve maximum extraction efficiency. As a result of complex experimental and analytical studies, a method for obtaining a thick licorice root extract has been proposed. Mechanical and circulating mixing of the extraction mixture increases the rate of internal heat and mass transfer and mass transfer at the interface during extraction, contributing to the formation of a developed phase contact surface and its renewal through convective diffusion processes. The proposed technology is characterized by environmental safety, since water is used as an extractant, and the use of microwave radiation reduces energy consumption. The resulting extract meets the requirements of the state standard and is highly effective. The results of the conducted research open up prospects for the wide application of this technology in the food industry.
About the Authors
E. V. SokolovaRussian Federation
assistant, Department of Technological Machines and Equipment, Tatishchev St., Bldg. 16/1, Astrakhan, Russia, 414056
Y. A. Maksimenko
Dr. Sci. (Engin.), professor, Department of Technological Machines and Equipment, Tatishchev St., Bldg. 16/1, Astrakhan, Russia, 414056
O. I. Konnova
assistant, Department of Technology of Goods and Commodity Science, Tatishchev St., Bldg. 16/1, Astrakhan, Russia, 414056
References
1. Babich O.O., Ulrikh E.V., Larina V.V., Bakhtiyarova A. Kh. Study of the composition and properties of Glycyrrhiza Glabra extracts grown in the Kaliningrad region and the prospects for its use // Food Systems. 2022. Vol. 5. no. 3. pp. 261–270. (in Russian).
2. Yan B., Hou J., Li W., Luo L. A review on the plant resources of important medicinal licorice // Journal of Ethnopharmacology. 2023. Vol. 301. pp. 115823. doi:10.1016/j.jep.2022.115823
3. Technical Regulations of the Customs Union TR CU 029/2012 Safety Requirements for Food Additives, Flavorings and Processing Aids. (in Russian).
4. Sridhar A., Vaishampayan V., Senthil Kumar P., Ponnuchamy M. Extraction techniques in food industry: Insights into process parameters and their optimization // Food Chem Toxicol. 2022. Vol. 166. pp. 113207. doi:10.1016/j.fct.2022.113207
5. Pavankumar R. M., Anet R. J., Shalini S. A. Green, environment-friendly and sustainable techniques for extraction of food bioactive compounds and waste valorization // Trends in Food Science & Technology. 2022. Vol. 128. pp. 296–315. doi:10.1016/j.tifs.2022.08.016
6. Khabibrakhmanova V.R., Sysoeva M.A., Khaled Sh. M., Gabdrakhmanova A.R. Selection of an extractant to increase the yield of triterpenoid substances and flavonoids from raw materials and licorice root meal (Glycyrrhizae Radices) // Issues of Biological, Medical and Pharmaceutical Chemistry. 2016. Vol. 19. no. 11. pp. 16–21. (in Russian).
7. Kvasenkov O.I., Tyuryukov A.B. Method of production of dry licorice extract. Patent RF, no. 2253463, 2005. (in Russian).
8. Butova S.N., Salnikova V.A., Shchegoleva I.D. Method for producing a saponin-containing extract. Patent RF, no. 2678840, 2019. (in Russian).
9. He Fei, Xin Xuelei, Wu Tao, Cheng Zhen et al. Preparation method and application of glycyrrhiza glabra extract. Patent CN, no. 113813300, 2021.
10. Pavlova L.V., Platonov I.A., Kurkin V.A., Novikova E.A. et al. Determination of glycyrrhizic acid in licorice roots by HPLC with subcritical extraction // Analytics and control. 2018. Vol. 22. no. 3. pp. 229–235. (in Russian).
11. Chen Jianle, Wang Qi, Ye Xingqian, Kwak Dong-Ki et al. Combined extraction method for functional factors of liquorice. Patent CN, no. 116554257, 2023.
12. State Standart 22840–77. Licorice root extract. Specifications. Moscow: Standartinform, 6 p. (in Russian).
13. State Standart 22839–88. Licorice roots and rhizomes. Specifications. Moscow: Standartinform, 4 p. (in Russian).
14. Ushakova N.F., Kopysova T.S., Kasatkin V.V., Kudryashova A.G. Experience in using microwave energy in food production // Food industry. 2013. no. 10. pp. 30–32. (in Russian).
15. Karami Z., Emam-Djomeh Z., Mirzaee H.A., Khomeiri M. et al. Optimization of microwave assisted extraction (MAE) and soxhlet extraction of phenolic compound from licorice root //Journal of food science and technology. 2015. Vol. 52. pp. 3242-3253.
16. Saidov S. S., Karimov R. K., Tadjibayeva M. R., Doniyarov G. T. et al. Optimization of licorice root extraction process // Universum: technical sciences. 2023. no.6-3 (111). pp. 61-66. (in Russian).
17. Lisovoy V. V., Pershakova T. V., Kornen N. N., Achmiz A.D. et al. The use of microwave EMF in technologies for processing plant raw materials and secondary resources // KubGAU Scientific Journal. 2016. no.118. pp. 1350-1362. (in Russian).
18. Jang S., Lee A. Y., Lee A. R., Choi G. et al. Optimization of ultrasound-assisted extraction of glycyrrhizic acid from licorice using response surface methodology // Integrative medicine research. 2017. Vol. 6. no. 4. pp. 388-394.
19. Ciganović P., Jakimiuk K., Tomczyk M., Zovko Končić M. Glycerolic licorice extracts as active cosmeceutical ingredients: Extraction optimization, chemical characterization, and biological activity //Antioxidants. 2019. Vol. 8. no. 10. pp. 445.
20. Giahi E., Jahadi M., Khosravi-Darani K. Enzyme-assisted extraction of glycyrrhizic acid from licorice roots using heat reflux and ultrasound methods // Biocatalysis and Agricultural Biotechnology. 2021. Vol. 33. pp. 101953.
Review
For citations:
Sokolova E.V., Maksimenko Y.A., Konnova O.I. Intensification of the extraction process in the production of licorice root extract. Proceedings of the Voronezh State University of Engineering Technologies. 2024;86(4):185-190. (In Russ.) https://doi.org/10.20914/2310-1202-2024-4-185-190